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Lebrini, M.; Robert, F.; Vezin, H.; Roos, C. |
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Title |
Electrochemical and quantum chemical studies of some indole derivatives as corrosion inhibitors for C38 steel in molar hydrochloric acid |
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Journal Article |
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Year |
2010 |
Publication |
Corrosion Science |
Abbreviated Journal |
Corrosion Sci. |
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Volume |
52 |
Issue |
10 |
Pages |
3367-3376 |
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Keywords |
Steel; EIS; Raman spectroscopy; Polarization; Acid inhibition |
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Abstract |
A comparative study of 9H-pyrido[3,4-b]indole (norharmane) and 1-methyl-9H-pyrido[3,4-b]indole (harmane) as inhibitors for C38 steel corrosion in 1 M HCl solution at 25 degrees C was carried out. Potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) techniques were applied to study the metal corrosion behavior in the absence and presence of different concentrations of these inhibitors. The OCP as a function of time were also established. Cathodic and anodic polarization curves show that norharmane and harmane are a mixed-type inhibitors. Adsorption of indole derivatives on the C38 steel surface, in 1 M HCl solution, follows the Langmuir adsorption isotherm model. The Delta G degrees(ads) values were calculated and discussed. The potential of zero charge (PZC) of the C38 steel in inhibited solution was studied by the EIS method, and a mechanism for the adsorption process was proposed. Raman spectroscopy confirmed that indole molecules strongly adsorbed onto the steel surface. The electronic properties of indole derivates, obtained using the AM1 semi-empirical quantum chemical approach, were correlated with their experimental efficiencies using the linear resistance model (LR). (C) 2010 Elsevier Ltd. All rights reserved. |
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[Robert, F.; Roos, C.] UAG UMR ECOFOG, Lab Mat & Mol Milieu Amazonien, Cayenne 97337, French Guiana, Email: christophe.roos@guyane.univ-ag.fr |
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PERGAMON-ELSEVIER SCIENCE LTD |
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0010-938X |
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ISI:000281315500026 |
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EcoFoG @ eric.marcon @ |
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44 |
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Lebrini, M.; Robert, F.; Roos, C. |
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Title |
Inhibition Effect of Alkaloids Extract from Annona Squamosa Plant on the Corrosion of C38 Steel in Normal Hydrochloric Acid Medium |
Type |
Journal Article |
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Year |
2010 |
Publication |
International Journal of Electrochemical Science |
Abbreviated Journal |
Int. J. Electrochem. Sci. |
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Volume |
5 |
Issue |
11 |
Pages |
1698-1712 |
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Keywords |
Plant extract; corrosion inhibitors; C38 steel; acidic media; adsorption |
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In this work, an alkaloids extract from Annona squamosa plant have been studied as possible corrosion inhibitor for C38 steel in molar hydrochloric acid (1 M HCl). Potentiodynamic polarization and AC impedance methods have been used. The corrosion inhibition efficiency increases on increasing plant extract concentration. Polarisation studies showed that Annona squamosa extract was mixed-type inhibitor in 1 M HCl. The inhibition efficiency of Annona squamosa extract was temperature-dependent and its addition led to an increase of the activation corrosion energy revealing a physical adsorption between the extract and the metal surface. The adsorption of the Annona squamosa extract followed Langmuir's adsorption isotherm. The inhibitive effect of Annona squamosa is ascribed to the presence of organic compounds in the extract. The examined extract is considered as non-cytotoxic substance. |
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[Lebrini, M.] CNRS 8172 UMR ECOFOG, Lab Mat & Mol Milieu Amazonien, Cayenne 97337, French Guiana, Email: florent.robert@guyane.univ-ag.fr |
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ELECTROCHEMICAL SCIENCE GROUP |
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1452-3981 |
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ISI:000283999000015 |
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EcoFoG @ eric.marcon @ |
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20 |
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Lebrini, M.; Robert, F.; Roos, C. |
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Title |
Alkaloids Extract from Palicourea guianensis Plant as Corrosion Inhibitor for C38 Steel in 1 M Hydrochloric Acid Medium |
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Journal Article |
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Year |
2011 |
Publication |
International Journal of Electrochemical Science |
Abbreviated Journal |
Int. J. Electrochem. Sci. |
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6 |
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3 |
Pages |
847-859 |
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Keywords |
Palicourea guianensis; corrosion inhibitors; C38 steel; acidic media; adsorption |
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Corrosion inhibition effect of alkaloids extract from Palicourea guianensis plant (AEPG) on C38 tell in 1 M HCl medium has been investigated by potentiodynamic polarization and electrochemical impedance spectroscopy. The polarization studies that AEPG acts as mixed-type inhibitor. The electrochemical impedance spectroscopy showed that the charge transfer resistance increases and the double layer capacitance decreases on increasing plant extract concentration. The inhibition efficiency of the extract obtained from impedance and polarization measurements was in a good agreement and was found to increase with increasing concentration of the extract. Inhibition efficiency of 89% was achieved with 100 mg L-1 of AEPG at 25 degrees C. The obtained results showed that, the Palicourea guianensis extract could serve as an effective inhibitor for the corrosion of steel in acid media. The adsorption of AEPG obeys the Langmuir adsorption isotherm. |
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[Lebrini, M.; Robert, F.; Roos, C.] UAG UMR ECOFOG, Lab Mat & Mol Milieu Amazonien, Cayenne 97337, French Guiana, Email: florent.robert@guyane.univ-ag.fr |
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Electrochemical Science Group |
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1452-3981 |
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ISI:000287820500026 |
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EcoFoG @ webmaster @ |
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298 |
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Author |
Lebrini, M.; Robert, F.; Roos, C. |
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Title |
Adsorption properties and inhibition of C38 steel corrosion in hydrochloric solution by some indole derivates: Temperature effect, activation energies, and thermodynamics of adsorption |
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Journal Article |
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Year |
2013 |
Publication |
International Journal of Corrosion |
Abbreviated Journal |
Int. J. Corros. |
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2013 |
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Article ID 139798 |
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13 |
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Abstract |
The corrosion rates in the presence of some indole derivates, namely, 9H-pyrido[3,4-b]indole (norharmane) and 1-methyl-9H-pyrido[3,4-b]indole (harmane), as inhibitors of C38 steel corrosion inhibitor in 1 M HCl solution, were measured by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) techniques, in the range of temperatures from 25 to 55 °C. Results obtained revealed that the organic compounds investigated have inhibiting properties for all temperatures. The inhibition was assumed to occur via adsorption of the indole molecules on the metal surface. Adsorption of indole derivates was found to follow the Langmuir isotherm. The apparent activation energies, enthalpies, and entropies of the dissolution process and the free energies and enthalpies for the adsorption process were determined by potentiodynamic polarization and electrochemical impedance. The fundamental thermodynamic functions were used to collect important information about indole inhibitory behaviour. © 2013 M. Lebrini et al. |
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Laboratoire Matériaux et Molécules en Milieu Amazonien, UAG-UMR ECOFOG, Campus Trou Biran, 97337 Cayenne, French Guiana |
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Export Date: 4 July 2013; Source: Scopus; Art. No.: 139798 |
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EcoFoG @ webmaster @ |
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495 |
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Lebrini, M.; Robert, F.; Lecante, A.; Roos, C. |
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Title |
Corrosion inhibition of C38 steel in 1 M hydrochloric acid medium by alkaloids extract from Oxandra asbeckii plant |
Type |
Journal Article |
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Year |
2011 |
Publication |
Corrosion Science |
Abbreviated Journal |
Corrosion Sci. |
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Volume |
53 |
Issue |
2 |
Pages |
687-695 |
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Keywords |
Steel; EIS; Polarization; Raman spectroscopy; Acid inhibition |
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The inhibition effect of alkaloids extract from Oxandra asbeckii plant (OAPE) on the corrosion of C38 steel in 1 M hydrochloric acid solution has been investigated by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The corrosion inhibition efficiency increases on increasing plant extracts concentration. Cathodic and anodic polarization curves show that OAPE is a mixed-type inhibitor. The effect of temperature on the corrosion behavior of C38 steel in 1 M HCl with and without addition of plant extract was studied in the temperature range 25-55 degrees C. The thermodynamic functions of dissolution and adsorption processes were calculated from experimental polarization data and the interpretation of the results are given. The adsorption of this plant extract on the C38 steel surface obeys the Langmuir adsorption isotherm. Surface analysis (Raman) was also carried out to establish the corrosion inhibitive property of this plant extract in HCl solution. (C) 2010 Elsevier Ltd. All rights reserved. |
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[Robert, F.; Lecante, A.; Roos, C.] UAG UMR ECOFOG, Lab Mat & Mol Milieu Amazonien, Cayenne 97337, French Guiana, Email: christophe.roos@guyane.univ-ag.fr |
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Pergamon-Elsevier Science Ltd |
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0010-938x |
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ISI:000287004700021 |
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EcoFoG @ webmaster @ |
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299 |
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Lebrini, M.; Robert, F.; Blandinieres, P.A.; Roos, C. |
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Title |
Corrosion Inhibition by Isertia coccinea Plant Extract in Hydrochloric Acid Solution |
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Journal Article |
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Year |
2011 |
Publication |
International Journal of Electrochemical Science |
Abbreviated Journal |
Int. J. Electrochem. Sci. |
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Volume |
6 |
Issue |
7 |
Pages |
2443-2460 |
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Keywords |
Isertia coccinea; corrosion inhibitors; C38 steel; acidic media; adsorption |
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The effect of alkaloids extracted from Isertia coccinea plant (AEIC) on the corrosion of C38 steel in 1 M hydrochloric acid was investigated by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques. Potentiodynamic polarization curves indicated that the extract behave as mixed-type inhibitor. The experimental data obtained from EIS method show a frequency distribution and therefore a modelling element with frequency dispersion behaviour, a constant phase element (CPE) has been used. The inhibition efficiencies of the extract calculated by three methods show the same tendency. Inhibition was found to increase with increasing concentration of the plant extract. The results obtained show that the extract solution of the plant could serve as an effective inhibitor for the corrosion of C38 steel in hydrochloric acid solution. The apparent activation energy of the process taking place in inhibitor presence was determined on the ground of four temperature values in the range from 25 degrees C to 55 degrees C using the data obtained by two independent methods. Theoretical fitting of different isotherms, Langmuir, Temkin and Frunkin, were tested to clarify the nature of adsorption. |
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[Lebrini, M.; Robert, F.; Blandinieres, P. A.; Roos, C.] UAG UMR ECOFOG, Lab Mat & Mol Milieu Amazonien, Cayenne 97337, French Guiana, Email: florent.robert@guyane.univ-ag.fr |
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Electrochemical Science Group |
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1452-3981 |
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ISI:000292331400014 |
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EcoFoG @ webmaster @ |
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324 |
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Lebrini, M.; Mbomekallé, I.M.; Dolbecq, A.; Marrot, J.; Berthet, P.; Ntienoue, J.; Sécheresse, F.; Vigneron, J.; Etcheberry, A. |
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Manganese(III)-containing wells-dawson sandwich-type polyoxometalates: Comparison with their manganese(II) counterparts |
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Journal Article |
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2011 |
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Inorganic Chemistry |
Abbreviated Journal |
Inorg. Chem. |
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50 |
Issue |
14 |
Pages |
6437-6448 |
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We present the synthesis and structural characterization, assessed by various techniques (FTIR, TGA, UV-vis, elemental analysis, single-crystal X-ray diffraction for three compounds, magnetic susceptibility, and electrochemistry) of five manganese-containing Wells-Dawson sandwich-type (WDST) complexes. The dimanganese(II)-containing complex, [Na2(H2O) 2MnII2(As2W15O 56)2]18- (1), was obtained by reaction of MnCl2 with 1 equiv of [As2W15O 56]12- in acetate medium (pH 4.7). Oxidation of 1 by Na2S2O8 in aqueous solution led to the dimanganese(III) complex [Na2(H2O)2Mn III2(As2W15O56) 2]16- (2), while its trimanganese(II) homologue, [Na(H2O)2MnII(H2O)Mn II2(As2W15O56) 2]17- (3), was obtained by addition of ca. 1 equiv of MnCl2 to a solution of 1 in 1 M NaCl. The trimanganese(III) and tetramanganese(III) counterparts, [MnIII(H2O)Mn III2(As2W15O56) 2]15- (4) and [MnIII2(H 2O)2MnIII2(As2W 15O56)2]12- (6), are, respectively, obtained by oxidation of aqueous solutions of 3 and [MnII2(H2O)2MnII2(As 2W15O56)2]16- (5) by Na2S2O8. Single-crystal X-ray analyses were carried out on 2, 3, and 4. BVS calculations and XPS confirmed that the oxidation state of Mn centers is +II for complexes 1, 3, and 5 and +III for 2, 4, and 6. A complete comparative electrochemical study was carried out on the six compounds cited above, and it was possible to observe the distinct redox steps MnIV/III and MnIII/II. Magnetization measurements, as a function of temperature, confirm the presence of antiferromagnetic interactions between the Mn ions in these compounds in all cases with the exception of compound 2. © 2011 American Chemical Society. |
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Laboratoire de Physico-Chimie de L'Etat Solide, ICMMO, Université Paris-Sud, Bâtiment 410, 91405 Orsay Cedex, France |
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00201669 (Issn) |
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Export Date: 21 October 2011; Source: Scopus; Coden: Inoca; doi: 10.1021/ic102237x; Language of Original Document: English; Correspondence Address: Mbomekallé, I.M.; Institut Lavoisier de Versailles, UMR 8180, CNRS Université de Versailles Saint-Quentin, 45 Avenue des Etats-Unis, 78035 Versailles Cedex, France; email: israel.mbomekalle@chimie.uvsq.fr |
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EcoFoG @ webmaster @ |
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346 |
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Leba, L.-J.; Popovici, J.; Estevez, Y.; Pelleau, S.; Legrand, E.; Musset, L.; Duplais, C. |
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Antiplasmodial activities of dyes against Plasmodium falciparum asexual and sexual stages: Contrasted uptakes of triarylmethanes Brilliant green, Green S (E142), and Patent Blue V (E131) by erythrocytes |
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Journal Article |
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Year |
2017 |
Publication |
International Journal for Parasitology: Drugs and Drug Resistance |
Abbreviated Journal |
International Journal for Parasitology: Drugs and Drug Resistance |
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Volume |
7 |
Issue |
3 |
Pages |
314-320 |
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Antimalarial dyes; Brilliant green; Drug uptake; Food dyes; Transmission blocking; Triarylmethanes |
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The search for safe antimalarial compounds acting against asexual symptom-responsible stages and sexual transmission-responsible forms of Plasmodium species is one of the major challenges in malaria elimination programs. So far, among current drugs approved for human use, only primaquine has transmission-blocking activity. The discovery of small molecules targeting different Plasmodium falciparum life stages remains a priority in antimalarial drug research. In this context, several independent studies have recently reported antiplasmodial and transmission-blocking activities of commonly used stains, dyes and fluorescent probes against P. falciparum including chloroquine-resistant isolates. Herein we have studied the antimalarial activities of dyes with different scaffold and we report that the triarylmethane dye (TRAM) Brilliant green inhibits the growth of asexual stages (IC50 ≤ 2 μM) and has exflagellation-blocking activity (IC50 ≤ 800 nM) against P. falciparum reference strains (3D7, 7G8) and chloroquine-resistant clinical isolate (Q206). In a second step we have investigated the antiplasmodial activities of two polysulfonated triarylmethane food dyes. Green S (E142) is weakly active against P. falciparum asexual stage (IC50 ≃ 17 μM) whereas Patent Blue V (E131) is inactive in both antimalarial assays. By applying liquid chromatography techniques for the culture supernatant analysis after cell washings and lysis, we report the detection of Brilliant green in erythrocytes, the selective uptake of Green S (E142) by infected erythrocytes, whereas Patent Blue V (E131) could not be detected within non-infected and 3D7-infected erythrocytes. Overall, our results suggest that two polysulfonated food dyes might display different affinity with transporters or channels on infected RBC membrane. © 2017 The Authors |
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Research Unit of Genetics and Genomics of Insect Vectors Institut Pasteur, Paris, France |
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Export Date: 18 September 2017 |
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EcoFoG @ webmaster @ |
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765 |
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Leba, L.-J.; Musset, L.; Pelleau, S.; Estevez, Y.; Birer, C.; Briolant, S.; Witkowski, B.; Ménard, D.; Delves, M.J.; Legrand, E.; Duplais, C.; Popovici, J. |
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Use of Plasmodium falciparum culture-adapted field isolates for in vitro exflagellation-blocking assay |
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Journal Article |
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2015 |
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Malaria Journal |
Abbreviated Journal |
Malaria Journal |
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14 |
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234 |
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Background: A major requirement for malaria elimination is the development of transmission-blocking interventions. In vitro transmission-blocking bioassays currently mostly rely on the use of very few Plasmodium falciparum reference laboratory strains isolated decades ago. To fill a piece of the gap between laboratory experimental models and natural systems, the purpose of this work was to determine if culture-adapted field isolates of P. falciparum are suitable for in vitro transmission-blocking bioassays targeting functional maturity of male gametocytes: exflagellation. Methods: Plasmodium falciparum isolates were adapted to in vitro culture before being used for in vitro gametocyte production. Maturation was assessed by microscopic observation of gametocyte morphology over time of culture and the functional viability of male gametocytes was assessed by microscopic counting of exflagellating gametocytes. Suitability for in vitro exflagellation-blocking bioassays was determined using dihydroartemisinin and methylene blue. Results: In vitro gametocyte production was achieved using two isolates from French Guiana and two isolates from Cambodia. Functional maturity of male gametocytes was assessed by exflagellation observations and all four isolates could be used in exflagellation-blocking bioassays with adequate response to methylene blue and dihydroartemisinin. Conclusion: This work shows that in vitro culture-adapted P. falciparum field isolates of different genetic background, from South America and Southeast Asia, can successfully be used for bioassays targeting the male gametocyte to gamete transition, exflagellation. © 2015 Leba et al. |
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Department of Life Sciences, Imperial College, London, United Kingdom |
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Export Date: 16 July 2015 |
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EcoFoG @ webmaster @ |
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612 |
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Le Lann, C.; Roux, O.; Serain, N.; Van Alphen, J.J.M.; Vernon, P.; Van Baaren, J. |
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Thermal tolerance of sympatric hymenopteran parasitoid species: does it match seasonal activity? |
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Journal Article |
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2011 |
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Physiological Entomology |
Abbreviated Journal |
Physiol. Entomol. |
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36 |
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1 |
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21-28 |
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Climate change; critical thermal limits; CTmax; CTmin; dry mass; guild; hind tibia length; seasonal activities; surface to volume ratio |
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Abstract |
Climatic changes result in an increased in mean temperature and in a higher incidence of extreme weather events such as heat and cold waves. For ectotherms, such as insect parasitoids, the ability to remain active under extreme climatic conditions is a significant key to fitness. The body size of individuals, and in particular their surface to volume ratio, may play a role in their resistance to thermal conditions. The thermal tolerances are investigated of two closely-related sympatric parasitoid species [Aphidius avenae Haliday and Aphidius rhopalosiphi De Stefani-Perez (Hymenoptera: Aphidiinae)] that have a similar ecology but differ in body size and phenologies. The critical thermal limits of individuals are assessed in both sexes of each parasitoid species and the influence of surface volume ratios on their thermal tolerances. Aphidius avenae is less resistant to low temperatures and more resistant to high temperatures than A. rhopalosiphi. The lower surface to volume ratio of A. avenae individuals may help them to remain active in summer when experiencing heat waves. However, body size is not the sole factor that plays a role in differences of thermal tolerance between species and body size may not be an adaptation to extreme temperatures but rather a by-product of developmental regulation. Closely-related sympatric species from the same ecological guild can have different thermal tolerances that may allow them to occur within the same habitat. The present study also highlights the importance of clearly defining how to measure critical thermal limits to determine the thermal tolerance of a species. |
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[Le Lann, Cecile; Serain, Nelly; Van Alphen, Jacques J. M.; Vernon, Philippe; Van Baaren, Joan] Univ Rennes 1, UMR CNRS ECOBIO 6553, F-35042 Rennes, France, Email: cecile.lelann@univ-rennes1.fr |
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Wiley-Blackwell |
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0307-6962 |
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ISI:000287790900004 |
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EcoFoG @ webmaster @ |
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294 |
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